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Artículo

Development and characterization of microwave-assisted activated carbons from Parkinsonea aculeata wood

Nunell, Gisel VanesaIcon ; Fernandez, Maria EmiliaIcon ; Bonelli, Pablo RicardoIcon ; Cukierman, Ana LeaIcon
Fecha de publicación: 04/2016
Editorial: Springer
Revista: Adsorption
ISSN: 0929-5607
e-ISSN: 1572-8757
Idioma: Inglés
Tipo de recurso: Artículo publicado
Clasificación temática:
Otras Ingeniería Química

Resumen

Activated carbons from invasive Parkinsonia aculeata wood sawdust were developed by microwave assisted H3PO4 acid activation varying the radiation time (2–10 min). Their main physicochemical characteristics were determined, and compared with those of a sample previously obtained by conventional heating using the same precursor, chemical agent, and impregnation ratio. The activated carbons developed for radiation times of 5 and 10 min showed higher BET surface areas (~1300 m2/g) and total pore volume (1 cm3/g) than those obtained at 2 min (~710 m2/g) or by conventional heating (~970 m2/g). Microwave assisted activation also led to activated carbons with higher total amounts of acidic oxygen and basic functionalities in comparison with the sample arising from conventional heating. Phenol adsorption capacity for all the samples was also evaluated from determination of the adsorption isotherms and their proper description by the Freundlich model. The adsorption capacity for the activated carbons obtained at 5 and 10 min was almost twice that measured for the samples prepared at 2 min and by conventional heating, in agreement with the higher BET surface areas characterizing the former. Compared with conventional heating, the process assistance by microwave energy not only reduced operation time, but also improved the characteristics of the resulting activated carbons.
Palabras clave: Activated Carbon , H3po4 Acid Activation , Microwave Assistance , Phenol Adsorption
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info:eu-repo/semantics/openAccess Excepto donde se diga explícitamente, este item se publica bajo la siguiente descripción: Creative Commons Attribution-NonCommercial-ShareAlike 2.5 Unported (CC BY-NC-SA 2.5)
Identificadores
URI: http://hdl.handle.net/11336/59577
DOI: http://dx.doi.org/10.1007/s10450-016-9783-z
URL: https://link.springer.com/article/10.1007%2Fs10450-016-9783-z
Colecciones
Articulos(OCA CIUDAD UNIVERSITARIA)
Articulos de OFICINA DE COORDINACION ADMINISTRATIVA CIUDAD UNIVERSITARIA
Citación
Nunell, Gisel Vanesa; Fernandez, Maria Emilia; Bonelli, Pablo Ricardo; Cukierman, Ana Lea; Development and characterization of microwave-assisted activated carbons from Parkinsonea aculeata wood; Springer; Adsorption; 22; 3; 4-2016; 347-356
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