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dc.contributor.author
Abonia, Rodrigo
dc.contributor.author
Castillo, Juan
dc.contributor.author
Insuasty, Braulio
dc.contributor.author
Quiroga, Jairo
dc.contributor.author
Sortino, Maximiliano Andrés
dc.contributor.author
Nogueras, Manuel
dc.contributor.author
Cobo, Justo
dc.date.available
2018-06-26T23:20:37Z
dc.date.issued
2016-05
dc.identifier.citation
Abonia, Rodrigo; Castillo, Juan; Insuasty, Braulio; Quiroga, Jairo; Sortino, Maximiliano Andrés; et al.; Catalyst-, solvent- and desiccant-free three-component synthesis of novel C-2,N-3 disubstituted thiazolidin-4-ones; Elsevier; Arabian Journal of Chemistry; 5-2016
dc.identifier.issn
1878-5352
dc.identifier.uri
http://hdl.handle.net/11336/50218
dc.description.abstract
Herein it is provided an efficient, environmentally friendly and one-pot procedure for the synthesis of a library of new and diversely substituted 1,3-thiazolidin-4-ones in short reaction times and good yields through a solvent-, catalyst- and desiccant-free three-component process. Reactions proceeded by treatment of primary benzyl(aryl)amines with aromatic aldehydes (and ketones) and 2-mercaptoacetic acid acting as both reagent and self-catalyst. All reactions were performed in sand bath instead of the commonly used oil bath avoiding the generation of undesired volatile materials proceeding of the thermal decomposition of the oils. IR, Mass and NMR experiments as well as X-ray diffraction confirmed structures of the obtained products.
dc.format
application/pdf
dc.language.iso
eng
dc.publisher
Elsevier
dc.rights
info:eu-repo/semantics/openAccess
dc.rights.uri
https://creativecommons.org/licenses/by-nc-nd/2.5/ar/
dc.subject
2-Mercaptoacetic Acid
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Green Synthesis
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Multicomponent Reactions
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Primary Benzylamines
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Solvent-Free Conditions
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Thiazolidin-4-Ones
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Otras Ciencias Químicas
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Ciencias Químicas
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CIENCIAS NATURALES Y EXACTAS
dc.title
Catalyst-, solvent- and desiccant-free three-component synthesis of novel C-2,N-3 disubstituted thiazolidin-4-ones
dc.type
info:eu-repo/semantics/article
dc.type
info:ar-repo/semantics/artículo
dc.type
info:eu-repo/semantics/publishedVersion
dc.date.updated
2018-06-26T22:34:32Z
dc.journal.pais
Países Bajos
dc.journal.ciudad
Amsterdam
dc.description.fil
Fil: Abonia, Rodrigo. Universidad del Valle; Colombia
dc.description.fil
Fil: Castillo, Juan. Universidad de los Andes; Colombia. Universidad del Valle; Colombia
dc.description.fil
Fil: Insuasty, Braulio. Universidad del Valle; Colombia
dc.description.fil
Fil: Quiroga, Jairo. Universidad del Valle; Colombia
dc.description.fil
Fil: Sortino, Maximiliano Andrés. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Rosario; Argentina. Universidad Nacional de Rosario. Facultad de Ciencias Bioquímicas y Farmacéuticas. Departamento de Química Orgánica. Área Farmacognosia; Argentina
dc.description.fil
Fil: Nogueras, Manuel. Universidad de Jaén; España
dc.description.fil
Fil: Cobo, Justo. Universidad de Jaén; España
dc.journal.title
Arabian Journal of Chemistry
dc.relation.alternativeid
info:eu-repo/semantics/altIdentifier/doi/http://dx.doi.org/10.1016/j.arabjc.2016.11.016
dc.relation.alternativeid
info:eu-repo/semantics/altIdentifier/url/https://www.sciencedirect.com/science/article/pii/S1878535216302258


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