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dc.contributor.author
Suárez Gómez, A.
dc.contributor.author
Figueroa, Santiago Jose Alejandro
dc.contributor.author
Lamas, Diego Germán
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Cezar, Julio C.
dc.date.available
2018-04-11T17:29:44Z
dc.date.issued
2015-04
dc.identifier.citation
Suárez Gómez, A.; Figueroa, Santiago Jose Alejandro; Lamas, Diego Germán; Cezar, Julio C.; A crystallization and structural study of the compound Pb2V2O7 synthesized by a facile sol–gel-based chemical route; Springer; Journal of Sol-Gel Science and Technology; 75; 2; 4-2015; 291-297
dc.identifier.issn
0928-0707
dc.identifier.uri
http://hdl.handle.net/11336/41728
dc.description.abstract
In this work, we carried out the synthesis of lead(II) divanadate(V) by means of a soft chemistry reaction based on a sol–gel-derived route. The final organic precursor was heat treated (T = 400, 500, 600, 750 and 800 °C) and structurally analyzed for each temperature by taking into account the results of FTIR spectroscopy, synchrotron X-ray powder diffraction and X-ray absorption near-edge structure. As an overall result, we report a final compound with remarkable crystallographic and morphological qualities that seem to keep all its structural features in the temperature range 450–700 °C before the structure incongruently melts. As a highlight, the desired material was obtained following a highly reproducible, low-cost, low-temperature and quite straightforward chemical route. Besides, this synthesis route could also allow the appropriate integration of lead(II) divanadate(V) nanoparticles, or nanolayers, into more complex systems as well as the feasibility for being expanded to other materials.
dc.format
application/pdf
dc.language.iso
eng
dc.publisher
Springer
dc.rights
info:eu-repo/semantics/restrictedAccess
dc.rights.uri
https://creativecommons.org/licenses/by-nc-sa/2.5/ar/
dc.subject
Divanadates
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Synchrotron
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Pb2v2o7
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Sol Gel
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Nanoparticles
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Nano-materiales
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Nanotecnología
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INGENIERÍAS Y TECNOLOGÍAS
dc.title
A crystallization and structural study of the compound Pb2V2O7 synthesized by a facile sol–gel-based chemical route
dc.type
info:eu-repo/semantics/article
dc.type
info:ar-repo/semantics/artículo
dc.type
info:eu-repo/semantics/publishedVersion
dc.date.updated
2018-04-11T15:12:26Z
dc.identifier.eissn
1573-4846
dc.journal.volume
75
dc.journal.number
2
dc.journal.pagination
291-297
dc.journal.pais
Alemania
dc.journal.ciudad
Berlín
dc.description.fil
Fil: Suárez Gómez, A.. Universidad de Guadalajara; México
dc.description.fil
Fil: Figueroa, Santiago Jose Alejandro. Brazilian Center of Energy and Materials; Brasil. Consejo Nacional de Investigaciones Científicas y Técnicas; Argentina
dc.description.fil
Fil: Lamas, Diego Germán. Consejo Nacional de Investigaciones Científicas y Técnicas; Argentina. Universidad Nacional de San Martín. Escuela de Ciencia y Tecnología; Argentina
dc.description.fil
Fil: Cezar, Julio C.. Brazilian Center of Energy and Materials; Brasil
dc.journal.title
Journal of Sol-Gel Science and Technology
dc.relation.alternativeid
info:eu-repo/semantics/altIdentifier/doi/http://dx.doi.org/10.1007/s10971-015-3698-0
dc.relation.alternativeid
info:eu-repo/semantics/altIdentifier/url/https://link.springer.com/article/10.1007/s10971-015-3698-0


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