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dc.contributor.author Suárez Gómez, A.
dc.contributor.author Figueroa, Santiago Jose Alejandro
dc.contributor.author Lamas, Diego Germán
dc.contributor.author Cezar, Julio C.
dc.date.available 2018-04-11T17:29:44Z
dc.date.issued 2015-04
dc.identifier.citation Suárez Gómez, A.; Figueroa, Santiago Jose Alejandro; Lamas, Diego Germán; Cezar, Julio C.; A crystallization and structural study of the compound Pb2V2O7 synthesized by a facile sol–gel-based chemical route; Springer; Journal of Sol-Gel Science and Technology; 75; 2; 4-2015; 291-297
dc.identifier.issn 0928-0707
dc.identifier.uri http://hdl.handle.net/11336/41728
dc.description.abstract In this work, we carried out the synthesis of lead(II) divanadate(V) by means of a soft chemistry reaction based on a sol–gel-derived route. The final organic precursor was heat treated (T = 400, 500, 600, 750 and 800 °C) and structurally analyzed for each temperature by taking into account the results of FTIR spectroscopy, synchrotron X-ray powder diffraction and X-ray absorption near-edge structure. As an overall result, we report a final compound with remarkable crystallographic and morphological qualities that seem to keep all its structural features in the temperature range 450–700 °C before the structure incongruently melts. As a highlight, the desired material was obtained following a highly reproducible, low-cost, low-temperature and quite straightforward chemical route. Besides, this synthesis route could also allow the appropriate integration of lead(II) divanadate(V) nanoparticles, or nanolayers, into more complex systems as well as the feasibility for being expanded to other materials.
dc.format application/pdf
dc.language.iso eng
dc.publisher Springer
dc.rights info:eu-repo/semantics/restrictedAccess
dc.rights.uri https://creativecommons.org/licenses/by-nc-sa/2.5/ar/
dc.subject Divanadates
dc.subject Synchrotron
dc.subject Pb2V2O7
dc.subject Sol gel
dc.subject Nanoparticles
dc.subject.classification Nano-materiales
dc.subject.classification Nanotecnología
dc.subject.classification INGENIERÍAS Y TECNOLOGÍAS
dc.title A crystallization and structural study of the compound Pb2V2O7 synthesized by a facile sol–gel-based chemical route
dc.type info:eu-repo/semantics/article
dc.type info:ar-repo/semantics/artículo
dc.type info:eu-repo/semantics/publishedVersion
dc.date.updated 2018-04-11T15:12:26Z
dc.identifier.eissn 1573-4846
dc.journal.volume 75
dc.journal.number 2
dc.journal.pagination 291-297
dc.journal.pais Alemania
dc.journal.ciudad Berlín
dc.description.fil Fil: Suárez Gómez, A.. Universidad de Guadalajara; México
dc.description.fil Fil: Figueroa, Santiago Jose Alejandro. Brazilian Center of Energy and Materials; Brasil. Consejo Nacional de Investigaciones Científicas y Técnicas; Argentina
dc.description.fil Fil: Lamas, Diego Germán. Consejo Nacional de Investigaciones Científicas y Técnicas; Argentina. Universidad Nacional de San Martín. Escuela de Ciencia y Tecnología; Argentina
dc.description.fil Fil: Cezar, Julio C.. Brazilian Center of Energy and Materials; Brasil
dc.journal.title Journal of Sol-Gel Science and Technology
dc.relation.alternativeid info:eu-repo/semantics/altIdentifier/doi/http://dx.doi.org/10.1007/s10971-015-3698-0
dc.relation.alternativeid info:eu-repo/semantics/altIdentifier/url/https://link.springer.com/article/10.1007/s10971-015-3698-0
dc.conicet.fuente individual


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info:eu-repo/semantics/restrictedAccess Excepto donde se diga explícitamente, este item se publica bajo la siguiente descripción: Creative Commons Attribution-NonCommercial-ShareAlike 2.5 Unported (CC BY-NC-SA 2.5)