Artículo

Synthesis and structure of novel iodinated N-glycosyl-sulfonamides through Aza-Ferrier reaction of 2-substituted glycals

Rojas, Agustin HugoIcon ; Lafuente, María LeticiaIcon ; Echeverría, Gustavo AlbertoIcon ; Piro, Oscar EnriqueIcon ; Vetere, VirginiaIcon ; Ponzinibbio, AgustínIcon
Fecha de publicación: 03/09/2020
Editorial: Elsevier
Revista: Tetrahedron Letters
ISSN: 0040-4039
Idioma: Inglés
Tipo de recurso: Artículo publicado
Clasificación temática:

Resumen

We obtained a series of novel N-(2-iodo-2,3-dideoxy-2-en-glycopyranosides)-sulfonamides via the Aza-Ferrier rearrangement of protected-2-iodoglycals in good yields and high stereoselectivity. Their structure and conformation features were determined by NMR. Moreover, we report here the first in detail structure analysis by X-ray diffraction techniques of a 2-iodo-pseudoglycal.
Palabras clave: 2-IODOGLYCALS , AZA-FERRIER REARRANGEMENT , N-GLYCOSYL SULFONAMIDES , NMR SPECTROSCOPY , X-RAY DIFFRACTION
 
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info:eu-repo/semantics/restrictedAccess Excepto donde se diga explícitamente, este item se publica bajo la siguiente descripción: Creative Commons Attribution-NonCommercial-ShareAlike 2.5 Unported (CC BY-NC-SA 2.5)
Identificadores
URI: http://hdl.handle.net/11336/140361
URL: https://linkinghub.elsevier.com/retrieve/pii/S0040403920307498
DOI: http://dx.doi.org/10.1016/j.tetlet.2020.152282
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Articulos(CINDECA)
Articulos de CENTRO DE INV EN CS.APLICADAS "DR.JORGE J.RONCO"
Citación
Rojas, Agustin Hugo; Lafuente, María Leticia; Echeverría, Gustavo Alberto; Piro, Oscar Enrique; Vetere, Virginia; et al.; Synthesis and structure of novel iodinated N-glycosyl-sulfonamides through Aza-Ferrier reaction of 2-substituted glycals; Elsevier; Tetrahedron Letters; 61; 36; 03-9-2020; 1-5
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